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Surface reduction of solid 3d transition metal compounds during x-ray photoelectron spectroscopy

✍ Scribed by B. Wallbank; C.E. Johnson; I.G. Main


Publisher
Elsevier Science
Year
1974
Tongue
English
Weight
500 KB
Volume
4
Category
Article
ISSN
0368-2048

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A method to prevent the reduction of CuO formed on Cu metal during x-ray photoelectron spectroscopy analysis is presented. When a bias voltage of -250 V was applied to the sample surface in the case of non-monochromatic Mg Ka,, irradiation, the reduction of CuO to the lower oxide (Cuz+ \* Cu+) was s