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Surface Hydrogelation of Thiolated Water-Soluble Copolymers on Gold

✍ Scribed by Nakayama, Y.; Nakamata, K.; Hirano, Y.; Goto, K.; Matsuda, T.

Book ID
127076000
Publisher
American Chemical Society
Year
1998
Tongue
English
Weight
169 KB
Volume
14
Category
Article
ISSN
0743-7463

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Supporting information for this article is available on the WWW under http://www.chemphyschem.org or from the author. Scheme 1. A) Synthesis of 1. a) 1. NaH, THF, 30 min, rt; 2. nBuLi, Γ€78 8C; 3. (Me 3 SiC 2 H 4 S) 2 , 12 h, Γ€78 8C to rt, (76 %); b) TBAF, THF, 4 h, rt, (92 %); c) DMTrCl, DMAP, pyrid