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Supramolecular Assembly of Dendritic Polymers Elucidated by 1 H and 13 C Solid-State MAS NMR Spectroscopy

✍ Scribed by Rapp, Almut; Schnell, Ingo; Sebastiani, Daniel; Brown, Steven P.; Percec, Virgil; Spiess, Hans Wolfgang

Book ID
125996731
Publisher
American Chemical Society
Year
2003
Tongue
English
Weight
522 KB
Volume
125
Category
Article
ISSN
0002-7863

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Order parameters describing conformational exchange processes on the nanosecond to microsecond timescale can be obtained from powder patterns in solid-state NMR (SSNMR) experiments. Extensions of these experiments to magic-angle spinning (MAS) based high-resolution experiments have been demonstrated