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Sulfuric Acid from Sulfur Trioxide and Water—A Surprisingly Complex Reaction

✍ Scribed by Prof. Dr. Ralf Steudel

Book ID
101555143
Publisher
John Wiley and Sons
Year
1995
Tongue
English
Weight
311 KB
Volume
34
Category
Article
ISSN
0044-8249

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Reactions of alkenoic acids with sulfur
Reactions of alkenoic acids with sulfur trioxide; sulfonation and sulfo-lactonization
✍ Ruud M. Schonk; B. H. Bakker; H. Cerfontain 📂 Article 📅 2010 🏛 Elsevier Science 🌐 English ⚖ 882 KB

## Abstract The reactions of the alkenoic acid derivatives 1a–19a with sulfur trioxide were studied in the temperature range −60 to 25°C using dichloromethane as solvent and 1.5 equiv. of dioxane as reactivity moderator. The alkenoic acids 13a and 14a, having a ‐(CH~2~)~4~‐ and ‐(CH~2~)~7~‐ linkage