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Substrate-Controlled Asymmetric Total Synthesis of (+)-Microcladallene B with a Bromination Strategy Based on a Nucleophile-Assisting Leaving Group

✍ Scribed by Janghyun Park; Byungsook Kim; Hyoungsu Kim; Sanghee Kim; Deukjoon Kim

Publisher: John Wiley and Sons
Year: 2007
Tongue: English
Weight: 143 KB
Volume: 119
Category: Article
ISSN: 0044-8249
DOI: 10.1002/ange.200700854

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Substrate-Controlled Asymmetric Total Sy

Substrate-Controlled Asymmetric Total Synthesis of (+)-Microcladallene B with a Bromination Strategy Based on a Nucleophile-Assisting Leaving Group

✍ Janghyun Park; Byungsook Kim; Hyoungsu Kim; Sanghee Kim; Deukjoon Kim 📂 Article 📅 2007 🏛 John Wiley and Sons 🌐 English ⚖ 144 KB 👁 2 views

Scheme 1. Retrosynthetic analysis of (+)-microcladallene B (1). PMB = p-methoxybenzyl. Scheme 2. Dianion alkylation of hydroxyamides. Bn = benzyl, HMDS = hexamethyldisilazide, TIPS = triisopropylsilyl.