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Study on phenolic resin beads: Effect of reaction parameters on the properties of polymeric beads

โœ Scribed by Smriti Shrivastava; Avanish Kumar Srivastava; Beer Singh; D. Shah; A. K. Verma; P. K. Gutch

Publisher
John Wiley and Sons
Year
2011
Tongue
English
Weight
781 KB
Volume
123
Category
Article
ISSN
0021-8995

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โœฆ Synopsis

Abstract

Wellโ€sized spherical beads of phenolic resin (0.3โ€“1.2 mm) with an extremely high compressive strength (>8 kg/1.0 mm bead) and hardness (>98%) were synthesized via suspension polymerization of phenol and formaldehyde. Barium hydroxide was used as a catalyst (1.68โ€“10.13 wt %) to get larger size of resin beads. Poly(vinyl alcohol) (5.0โ€“12.5 wt %) and hexamethylene tetramine were used as stabilizing agent and crosslinking agent, respectively. Comprehensive studies elucidated a specific relation between the reaction parameters and properties of the resin beads. Yield was found proportional to catalyst concentration and inversely proportional to stabilizing agent concentration. Particle size distribution curves got contracted and shifted toward a lower size range with higher concentration of catalyst and stabilizing agent. ยฉ 2011 Wiley Periodicals, Inc. J Appl Polym Sci, 2012

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