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Study of radical cations ofcis- andtrans-decalin in nonpolar solutions by the MARY and optically detected ESR spectroscopy

โœ Scribed by B. M. Tadjikov; D. V. Stas; Yu. N. Molin

Book ID
105596308
Publisher
Springer
Year
1997
Tongue
English
Weight
497 KB
Volume
46
Category
Article
ISSN
1573-9171

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๐Ÿ“œ SIMILAR VOLUMES

Can both cis- and trans-isomers of the 9
Can both cis- and trans-isomers of the 9-decalyl radical be detected in solution by ESR spectroscopy?
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A ptevrous report that distinguishable ESR spectra can be obtained from CIS-and truns-Isomers of the 9-decalyl radical m liquid solution at low temperature is shown to be incorrect. Only one spectrum, assigned to the rrans-radtcal, is observable from etther CIS-or rruns-precursors In 1985 Lloyd and

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โœ Herbert Rubin; Hanns Fischer ๐Ÿ“‚ Article ๐Ÿ“… 1996 ๐Ÿ› John Wiley and Sons ๐ŸŒ German โš– 686 KB

All arrangements and procedures for steady-state and time-resolved ESR were as described in [4]. The radicals Me,C and Me3C02CCH, were generated by photolysis of the corresponding disubstituted ketones. These undergo type-I cleavage from a short-lived triplet state followed by a fast decarbonylation