## Abstract Micro capillary columns were successfully applied to liquid chromatography by employing the principles used in micro high performance liquid chromatography. Fundamental investigations on the use of capillary columns in LC were performed for the various column parameters. Good separation
Study of open-tubular micro-capillary liquid chromatography
β Scribed by Ishii, D. ;Tsuda, T. ;Hibi, K. ;Takeuchi, T. ;Nakanishi, T.
- Publisher
- John Wiley and Sons
- Year
- 1979
- Tongue
- English
- Weight
- 642 KB
- Volume
- 2
- Category
- Article
- ISSN
- 0935-6304
No coin nor oath required. For personal study only.
β¦ Synopsis
Abstract
Capillary columns in gas chromatography, first proposed by Golay [1,2], have become well established [3] which have extremely high column efficiencies and separabilities. Everyone could imagine it to be a great tool if such a kind of high efficiency column could be established in liquid chromatography (LC). Microcapillary liquid chromatography (MCLC) may be one way of achieving highβefficiency in terms of theoretical plates. Few papers were published in this field before 1976 [4β6], but more recently, after 1977 [7β15], this field has become one of topical interest in liquid chromatography. Temporarily there are two microcapillary liquid chromatography, that is: βopenβtubularβοΈ [7,8,10β15] and βpackedβοΈ [9] MCLC. In this presentation we focus on openβtubular microcapillary liquid chromatography and a review contemporary developments of ours and others.
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## Abstract The performance of etched borosilicate capillary columns with a bonded octadecyl stationary phase has been examined. Plate heights for three test compounds in columns with inner diameters between 6.5 and 14.6 ΞΌm were measured as a function of mobile phase velocity. The reduced plate hei