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Studies on the phosphorylation of LY303366

✍ Scribed by Uko E. Udodong; William W. Turner; Bret A. Astleford; Frank Brown Jr.; Marcella T. Clayton; Steven E. Dunlap; Scott A. Frank; John L. Grutsch; Lisa M. LaGrandeur; Daniel E. Verral; John A. Werner

Publisher: Elsevier Science
Year: 1998
Tongue: French
Weight: 183 KB
Volume: 39
Category: Article
ISSN: 0040-4039
DOI: 10.1016/s0040-4039(98)01294-5

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✦ Synopsis

Phosphorylation of LY303366 (1) was studied in THF and DMF. Benzyl phosphate 2 could be prepared in excellent yield using LiOH as the base. Both 2 and the derived phosphonic acid monosodium salt 3 were prone to undergo hydrolytic dephosphorylation.

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