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Studies on microgels, 3. Synthesis using living free radical polymerization

✍ Scribed by Simmi Abrol; Peter A. Kambouris; Mark G. Looney; David H. Solomon

Publisher: John Wiley and Sons
Year: 1997
Tongue: English
Weight: 309 KB
Volume: 18
Category: Article
ISSN: 1022-1336
DOI: 10.1002/marc.1997.030180901

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✦ Synopsis

Abstract

Microgels which are soluble crosslinked polymer networks have been prepared using the nitroxide living free radical polymerization methodology. When heated in the presence of tert‐butylstyrene and 1,4‐divinylbenzene, the alkoxyamine 1 derived from 2,2′‐azoisobutyronitrile (AIBN) afforded a high molecular weight soluble polymer which was shown by size exclusion chromatography in conjunction with an on‐line multi angle laser light scattering (MALLS) detector to have microgel properties.

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