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Strukturen und Moleküleigenschaften sterisch überfüllter Moleküle, 36. (E)-1,1,1,4,4,4-Hexakis(trimethylsilyl)-2-buten [(H3C)3Si]3C—HCCH—C[Si(CH3)3]3 und Bis[tris(trimethylsilyl)silyl]ethin [(H3C)3Si]3Si—C≡C—Si[Si(CH3)3]3

✍ Scribed by Bock, Hans ;Meuret, Jochen ;Schödel, Holger

Publisher
Wiley (John Wiley & Sons)
Year
1993
Tongue
English
Weight
840 KB
Volume
126
Category
Article
ISSN
0009-2940

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The reaction of InBr 3 with LiR\* ´(THF) n (R\* = ±C(SiMe 3 ) 3 , THF = OC 4 H 8 ) in a 1 : 1 molar ratio forms [Li(THF) 4 ][R\*InBr 3 ] in good yield. The properties and some spectroscopic data ( 1 H, 13 C, 29 Si, 7 Li±NMR, IR and Raman) of this trisyl-tribromoindate are given and the crystal struc