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Structures of two isomeric 17-picolinylidene derivatives of 5-androsten-16-ones

✍ Scribed by Stanković, S. ;Ribár, B. ;Miljković, D. ;Gaši, K. ;Courseille, C.

Book ID: 114505957
Publisher: International Union of Crystallography
Year: 1989
Tongue: English
Weight: 550 KB
Volume: 45
Category: Article
ISSN: 0108-2701
DOI: 10.1107/s010827018801162x

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## Abstract A method has been described for the synthesis of tritiated [7‐^3^H]‐3β,16β‐dihydroxy‐5‐androsten‐17‐one of high specific activity starting from [7‐^3^H]‐5‐androsten‐17‐one. The identity of the radioactive steroid was established by thin layer chromato‐graphy, gas chromatography and gas