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Structures of 3'-azido-2',3'-dideoxy-1-β-d-threo-pentofuranosyluracil and 3'-azido-2',3'-dideoxy-1-β-d-erythro-pentofuranosyluracil

✍ Scribed by Low, J. N. ;Tollin, P.

Book ID
114506081
Publisher
International Union of Crystallography
Year
1989
Tongue
English
Weight
313 KB
Volume
45
Category
Article
ISSN
0108-2701

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## Abstract The α,β‐unsaturated D‐sugar aldehyde 2, prepared from tri‐__O__‐acetyl‐D‐glucal, was converted into 1‐__O__‐acetyl‐3‐azido‐2,3‐dideoxy‐α‐D‐__arabino__‐pyranose (3) by reaction with sodium azide in a mixture of acetic acid and water followed by acetylation. Reaction of 3 with silylated p