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Structure-toxicity relationships of 1-substituted-4-alkyl-2,6,7-trioxabicyclo[2.2.2.]octanes

✍ Scribed by Dean S. Milbrath; Judith L. Engel; John G. Verkade; John E. Casida

Book ID: 116072510
Publisher: Elsevier Science
Year: 1979
Tongue: English
Weight: 552 KB
Volume: 47
Category: Article
ISSN: 0041-008X
DOI: 10.1016/0041-008x(79)90323-5

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The metalation of (El-l-(2-chlorovinyl)-or (E)-1-(2-bromovinyl)-4-methyl-2,6,7-trioxabicyclo[2.2.2]octane with tert-butyllithium produced an unsaturated homoenolate anion equivalent which intercepted alkyl halides, aldehydes, ketones, and lactones to afford 8-alkylated or 8-acylated orthoesters, whi