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Structure-biodegradability relationships of insecticidal 1,4-disubstituted-2,6,7-trioxabicyclo[2.2.2]octanes

✍ Scribed by Cole, Loretta M.; Sanders, Mark; Palmer, Christopher J.; Casida, John E.

Book ID: 127307782
Publisher: American Chemical Society
Year: 1991
Tongue: English
Weight: 772 KB
Volume: 39
Category: Article
ISSN: 0021-8561
DOI: 10.1021/jf00003a025

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The metalation of (El-l-(2-chlorovinyl)-or (E)-1-(2-bromovinyl)-4-methyl-2,6,7-trioxabicyclo[2.2.2]octane with tert-butyllithium produced an unsaturated homoenolate anion equivalent which intercepted alkyl halides, aldehydes, ketones, and lactones to afford 8-alkylated or 8-acylated orthoesters, whi