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Structure of patulolide a, a new macrolide from penicillium urticae mutants

✍ Scribed by Junichi Sekiguchi; Hironori Kuroda; Yasuhiro Yamada; Hirosuke Okada

Publisher
Elsevier Science
Year
1985
Tongue
French
Weight
125 KB
Volume
26
Category
Article
ISSN
0040-4039

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Chemoenzymatic Synthesis of (R)-(+)-Patu
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## Abstract (__R__)‐(+)‐Patulolide A [(__R__)‐1] was synthesized with an enantiomeric purity of almost 100% e.e. by a two‐step lipase‐catalyzed enantioselective hydrolysis of racemic thioketal acetate (±)‐11.

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An enantioselective synthesis of patulolide A (1). patulolide B (2). and pdtulolide C (3) from ethyl (R)-3-bydroxybutanoate is described. Recently Yamada and his co-workers isolated three new antimicrobial macrolides from the culture broth of Penicil- lium urticae mutant S11R59, named them patuloli

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