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Structure of cyclo-1,1',4,4'-bis(1,1,3,3-tetramethyl-1,3-disiloxanediyl)dibenzene

✍ Scribed by Abboud, K. A. ;Smith Jnr, D. W. ;Wagener, K. B.

Book ID: 114510205
Publisher: International Union of Crystallography
Year: 1993
Tongue: English
Weight: 441 KB
Volume: 49
Category: Article
ISSN: 0108-2701
DOI: 10.1107/s0108270193002331

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The title compound, C~18~H~14~Cl~3~NO~2~S~2~, was synthesized by the reaction of 1,1,2,4-tetrachloro-4-(4-methylphenylsulfanyl)-3-nitrobuta-1,3-diene with ethanedithiol. The butadiene unit is not completely planar as would be expected if the two double bonds were fully conjugated The torsion angle o