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Structure of cis-bicyclo[3.3.0]oct-3-ene-2,7-dione 7-(2,2-dimethyltrimethylene acetal)

✍ Scribed by Solans, X. ;Font-Altaba, M. ;Moyano, A. ;Carceller, E. ;Serratosa, F.

Book ID: 114503217
Publisher: International Union of Crystallography
Year: 1985
Tongue: English
Weight: 218 KB
Volume: 41
Category: Article
ISSN: 0108-2701
DOI: 10.1107/s0108270185008824

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The title compound, C~6~H~7~NO~2~, was synthesized from __cis__-1,2-cyclobutanedicarboxylic anhydride by reaction with ammonium acetate under microwave conditions. The crystal structure of the compound shows that the cyclobutane ring is planar with angles ranging from 89.64 (12) to 90.37 (12)°. The