Synthesis of d Transition Metal Sulfides
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M. Abboudi; A. Mosset
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Article
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1994
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Elsevier Science
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English
β 389 KB
Sulfides of six transition or post-transition metals have been prepared by decomposition of amorphous dithiooxamide complexes. The best procedure of pyrolysis corresponds to a heating at \(680^{\circ} \mathrm{C}\) under a dynamic vacuum during \(4 \mathrm{hr}\). This preparation, without any added s