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Structure of acetamidine, C2H6N2, at 108 K

✍ Scribed by Norrestam, R. ;Mertz, S. ;Crossland, I.


Book ID
114501785
Publisher
International Union of Crystallography
Year
1983
Tongue
English
Weight
338 KB
Volume
39
Category
Article
ISSN
0108-2701

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3a-BF4 To a wlution of I-BF, (0.46g. 1 mmol) in dichloromethane (5 mL) at ~ 50 c' wiis added palladium tetrakis(tripheny1phosphane) (0.86 g. 0 75 mmolj. After \tirriiig for 1X h a t 40 C. the solvent was removed in vacuo. and the reziduc w a \ washed several times with toluene andether to give 3a-BF