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Structure of a bis(η4-exocyclic-1,3-diene)Fe(CO)3 complex

Book ID
114505274
Publisher
International Union of Crystallography
Year
1988
Tongue
English
Weight
342 KB
Volume
44
Category
Article
ISSN
0108-2701

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## Experimental Section 3: Compound 4 [4] (80 mg, 0.075 mmol) and KC 8 (22 mg, 0.163 mmol) were placed in a reaction tube with a magnetic stirrer. Oxygen-free, dry THF (2 mL) was introduced into the reaction tube by vacuum transfer, and the reaction mixture was stirred at room temperature to produ