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Structure of 9-{2-[(4-imidazolyl)methylthio]ethyl}adenine

✍ Scribed by Takimoto-Kamimura, M. ;Takenaka, A. ;Sasada, Y. ;Ohki, M.

Book ID
114503790
Publisher
International Union of Crystallography
Year
1986
Tongue
English
Weight
312 KB
Volume
42
Category
Article
ISSN
0108-2701

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Synthesis of 9-(2-phosphonylmethoxy)ethy
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✍ U. J. Haynes; J. E. Swigor; J. J. Bronson 📂 Article 📅 1992 🏛 John Wiley and Sons 🌐 French ⚖ 153 KB

## Abstract The synthesis of [^14^C] PMEA (3) was achieved by coupling the sodium salt of 8‐[^14^C]adenine (1) with 2‐(diisopropyl‐phosphonymethoxy) ethanol methanesulfonate in N,N‐dimethylformamide at 100°C to provide the diisopropyl ester (2). Deesterification with bromotrimethylsilane in acetoni