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Structure of 1,8-bis(hydroxymethyl)naphthalene

✍ Scribed by Bennett, G. D. ;Fitzgerald, L. J. ;Gerkin, R. E.


Book ID
114509613
Publisher
International Union of Crystallography
Year
1993
Tongue
English
Weight
592 KB
Volume
49
Category
Article
ISSN
0108-2701

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A series of 1,8-bis(phosphino)naphthalenes 2 was prepared by treating 1,8-dilithionaphthalene with the appropriate chloro-or bromophosphines RRЈPX; R, RЈ ‫ס‬ Me (for 2a), iPr (for 2c), Cy (for 2d), Ph (for 2f); R ‫ס‬ tBu, RЈ ‫ס‬ Ph (for 2e) (X ‫ס‬ Cl) and R, RЈ ‫ס‬ Et; X ‫ס‬ Br (for 2b). The resulti