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Structure of 17β-hydroxy-1,4-androstadien-3-one monohydrate C19H26O2·H2O

✍ Scribed by Zdzisław Gałdecki; Paweł Grochulski; Zdzisław Wawrzak; Andrzej Szyczewski


Publisher
Springer
Year
1989
Tongue
English
Weight
228 KB
Volume
19
Category
Article
ISSN
1572-8854

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Preparation of 17β-hydroxy-[1ξ,2ξ-3H2]4,
✍ Clinton A. Taylor Jr.; Benjamin J. Danzo; Howard E. Smith 📂 Article 📅 1980 🏛 John Wiley and Sons 🌐 French ⚖ 277 KB 👁 1 views

## Abstract 17β‐Hydroxy‐[1ξ,2ξ‐^3^H~2~]4,6‐androstadien‐3‐one was prepared by the selective reduction of 17β‐hydroxy‐1,4,6‐androstatrien‐3‐one in benzene with tritium over 5% palladium on carbon. After purification by thin layer chromatography and high pressure liquid chromatography, the specific a