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Structure identification of terpene-type alcohols at microgram levels

โœ Scribed by Bierl-Leonhardt, B. A.; DeVilbiss, E. D.


Book ID
126290492
Publisher
American Chemical Society
Year
1981
Tongue
English
Weight
431 KB
Volume
53
Category
Article
ISSN
0003-2700

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A simple procedure is described in which micro-and submicrogram amounts of primary, secondary, and several tertiary alcohols can be acetylated. The alcohols, dissolved in a nonpolar solvent, contact a column of Celite charged with the mixed anhydride, acetyl methanesulfonate, contained in a melting-