𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Structure elucidation of the dye Acid Red 131: complete 1H, 13C and 15N NMR data assignment

✍ Scribed by Elisabetta Schievano; Ileana Menegazzo; Ester Marotta; Stefano Mammi

Publisher
John Wiley and Sons
Year
2011
Tongue
English
Weight
222 KB
Volume
49
Category
Article
ISSN
0749-1581

No coin nor oath required. For personal study only.

✦ Synopsis

Abstract

The chemistry of dyes and pigments is relevant to the textile industry, because of the importance to establish the best conditions for the finishing process and to understand the interactions among various compounds to yield the correct hue and nuances. For this reason, the molecular structure of a monoazo acid dye, C.I. Acid Red 131, was elucidated and characterized by homo‐ and hetero‐nuclear NMR, MS, IR and UV spectroscopy techniques. Copyright © 2011 John Wiley & Sons, Ltd.

📜 SIMILAR VOLUMES

Complete assignments of the 1H and 13C N
Complete assignments of the 1H and 13C NMR spectra of 15 limonoids
✍ Benjamín Rodríguez 📂 Article 📅 2003 🏛 John Wiley and Sons 🌐 English ⚖ 139 KB

## Abstract Unambiguous and complete assignments of ^1^H and ^13^C NMR chemical shifts for 15 limonoids, eight of them found in natural sources and seven other synthetic derivatives, are presented. The assignments are based on 2D shift‐correlated [^1^H,^1^H‐COSY, ^1^H,^13^C‐gHSQC‐^1^__J__(C,H), ^1^

Complete 1H and 13C NMR assignments of t
Complete 1H and 13C NMR assignments of the epimeric menthane-1-carboxylic acids
✍ Debra K. Dillner; Daniel D. Traficante 📂 Article 📅 2007 🏛 John Wiley and Sons 🌐 English ⚖ 93 KB

## Abstract Complete NMR analyses with full assignments for ^1^H and ^13^C NMR spectral data for both epimers of menthane‐1‐carboxylic acid are described. The NMR properties of the recently synthesized axial isomer had not been previously described, and through use of a variety of 1D and 2D techniq

Complete assignment of the 1H, 13C and 1
Complete assignment of the 1H, 13C and 15N spectra of bradykinin derivatives
✍ Oliver Zerbe; John H. Welsh; John A. Robinson; Wolf-Gang Von Philipsborn 📂 Article 📅 1992 🏛 John Wiley and Sons 🌐 English ⚖ 228 KB

## Abstract The complete assignment of the ^1^H, ^13^C and ^15^N spectra of bradykinin derivatives is presented. The proton assignments were performed using COSY, TOCSY and ROESY experiments, whereas the heteronuclei were assigned using inverse correlation experiments.

Complete 1H, 13C and 15N NMR assignment
Complete 1H, 13C and 15N NMR assignment of tirapazamine and related 1,2,4-benzotriazine N-oxides
✍ Maruta Boyd; Michael P. Hay; Peter D. W. Boyd 📂 Article 📅 2006 🏛 John Wiley and Sons 🌐 English ⚖ 183 KB

## Abstract ^1^H, ^13^C and ^15^N NMR measurements (1D and 2D including ^1^H^15^N gs‐HMBC) have been carried out on 3‐amino‐1, 2,4‐benzotriazine and a series of __N__‐oxides and complete assignments established. __N__‐Oxidation at any position resulted in large upfield shifts of the corresponding

Complete assignment of the 1H and 13C NM
Complete assignment of the 1H and 13C NMR spectra of the tetraisoprenylated benzophenone 15-epiclusianone
✍ M. H. dos Santos; T. J. Nagem; R. Braz-Filho; I. S. Lula; N. L. Speziali 📂 Article 📅 2001 🏛 John Wiley and Sons 🌐 English ⚖ 171 KB

## Abstract An NMR study of 15‐epiclusianone, 1‐benzoyl‐6‐hydroxy‐14,14‐dimethyl‐3,5,15‐tri(3‐methyl‐2‐butenyl)‐bicyclo[3.3.1]non‐1‐ene‐4,6‐dione (**1**), a novel tetraisoprenylated benzophenone isolated from pericarp of fruits of __Rheedia gardneriana__, is described. In addition to conventional 1

Total assignment of 1H and 13C NMR data
Total assignment of 1H and 13C NMR data for the sesquiterpene lactone 15-deoxygoyazensolide
✍ Vladimir Constantino Gomes Heleno; Antônio Eduardo Miller Crotti; Mauricio Gomes 📂 Article 📅 2004 🏛 John Wiley and Sons 🌐 English ⚖ 97 KB

## Abstract We describe a complete analysis of the ^1^H and ^13^C spectra of the anti‐inflamatory, schistossomicidal and trypanosomicidal sesquiterpene lactone 15‐deoxygoyazensolide. This lactone, with a structure similar to other important ones, was studied by NMR techniques such as COSY, HMQC, HM