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Structure determination of a ceramide pentadecasaccharide by two-dimensional J-resolved and J-correlated NMR spectroscopy

✍ Scribed by Janusz Dabrowski; Peter Hanfland

Book ID
115913180
Publisher
Elsevier Science
Year
1982
Tongue
English
Weight
247 KB
Volume
142
Category
Article
ISSN
0014-5793

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Two-dimensional shift-correlated (COSY) and J-resolved NMR spectroscopy was used to identify and assign resonance in the aliphatic region (0.8 to 4.5 ppm) of the 1H spectrum of acid extracts and tissue of rat brain. The chemical shift and spin-spin coupling constants of several resonances, which cou