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Structure Determination and Relative Properties of Novel Noncentrosymmetric Borates MM′4(BO3)3 (M: Na, M′: Ca and M: K, M′: Ca, Sr).

✍ Scribed by L. Wu; X. L. Chen; Y. P. Xu; Y. P. Sun

Publisher
John Wiley and Sons
Year
2006
Weight
10 KB
Volume
37
Category
Article
ISSN
0931-7597

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✍ Li Xu; Zhaohui Li; Huang Liu; Jinshun Huang; Qianer Zhang 📂 Article 📅 1997 🏛 John Wiley and Sons 🌐 English ⚖ 628 KB

A mixture of Na,MO,, M(CO),, FeC1,.6 H,O, and (EtCO),O was heated at 120 ' C to produce the heterooctanuclear clusters Na,Fe,[M,O,-(O,CEt),], (M = Mo, 1; W, 2). The bioxo-capped clusters Na[M,O,(O,CEt),] (M, = MOW,, W,) were treated with Fe-(CO),, Cr(CO),, and Mo(CO), in (EtCO),O at 120°C to afford