A particular method of continuous electrolysis through porous electrodes is described for the preparation of N-amino Z-methyl indoline by electroreduction of N-nitroso Z-methyl indoline. The process takes into account the instability of(i) the starting material in very acidic medium (reaction Z), (i
✦ LIBER ✦
Structure de la N-methyl-N-nitroso-N′-nitroguanidine et de la trimethyl nitroso UREE: Etude par RMN 15N
✍ Scribed by J.P. Gouesnard
- Publisher
- Elsevier Science
- Year
- 1983
- Tongue
- English
- Weight
- 423 KB
- Volume
- 96
- Category
- Article
- ISSN
- 0022-2860
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The two compounds were labelled by ^14^C on the hydroxyimino methyl group substituted on the 2 positions of the pyridinium ring. The convenient pyridinium lithiated intermediates were formylated with N‐methyl ^14^C‐formanilide. The hydroxyimino methyl groups were synthezised by reaction of the ^14^