Information concerning the internal structure of the layers in a glassy carbon is completed by the description of the layer stackings. This description is deduced from the X-ray 001 reflections and from the electron microscopy lattice imaging. These results are used to develop and refine a spatial s
Structural evolution of a glassy carbon as a result of thermal treatment between 1000 and 2700°c—I: Evolution of the layers
✍ Scribed by F. Rousseaux; D. Tchoubar
- Publisher
- Elsevier Science
- Year
- 1977
- Tongue
- English
- Weight
- 767 KB
- Volume
- 15
- Category
- Article
- ISSN
- 0008-6223
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✦ Synopsis
The structural evolution of a glassy carbon is studied by analysis of the X-ray diffraction two-dimensional lines. A strong anisotropy is found in the growth of the carbon layers and in their lattice distortions. The results are correlated with the carbonization mechanism of the polymer precursor. H(s) = J(s) -Fcm,o.b) f(s) where I(s) represents the experimental intensity normalized to one carbon atom and corrected from polarisation and absorption, F common is the Compton scattering factor of a covalent carbon corrected for the Breit-Dirac factor and f(s) is the coherent scattering factor for the same atom.
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