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Structural Characterization of Molybdenum(V) Species in Aqueous HCl Solutions

✍ Scribed by Mah, Vicky; Leung, Bonnie O.; Ross, Daniel; Jalilehvand, Farideh; Parvez, Masood; Aroca, Ricardo F.

Book ID
111926623
Publisher
American Chemical Society
Year
2007
Tongue
English
Weight
649 KB
Volume
46
Category
Article
ISSN
0020-1669

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Reduction of ammonium molybdate, (NH 4 ) 6 Mo 7 O 24 '4H 2 O, with hydroxylamine hydrochloride. NH 2 OH'HCl, at ambient temperature in aqueous solutions results in amorphous MoO 3 'nH 2 O oxide. Subsequent heat treatment of this oxide yields Mo 1؊ O 2 or a hydrogen molybdenum bronze, H x MoO 3 (x:1)