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Straightforward Microwave-Assisted Synthesis of 5,8-Disubstituted 5,6,8,9-Te­trahydro-4 H ,7 H -2,5,6a,8,9a-pentaazaphenalene-1,3-diones

✍ Scribed by García, Daniel; Jatczak, Martyna; Muylaert, Koen; De Coen, Laurens M.; Stevens, Christian V.


Book ID
120008761
Publisher
John Wiley and Sons
Year
2013
Tongue
English
Weight
664 KB
Volume
2013
Category
Article
ISSN
1434-193X

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✍ Bigdeli, M. Ali ;Mahdavinia, Gholam Hossein ;Amani, Vahid 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 646 KB

The title compound, C 23 H 25 BrO 3 , was synthesized by the reaction of p-bromobenzaldehyde with dimedone and HClO 4 / SiO 2 in EtOH. In the molecule, the dihydropyran ring adopts a boat conformation and the two cyclohexene rings are in a trans conformation.