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Sterically oriented synthesis and structure of new perphosphorylated resorcinarenes

✍ Scribed by V. I. Maslennikova; O. S. Serkova; T. V. Guzeeva; L. K. Vasyanina; K. A. Lysenko; V. V. Kopteva; E. E. Nifant’ev

Book ID: 111459578
Publisher: Springer
Year: 2008
Tongue: English
Weight: 298 KB
Volume: 78
Category: Article
ISSN: 1070-3632
DOI: 10.1134/s1070363208030092

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The acid-catalyzed (with HCl) condensation reactions of resorcinol ( ) with 1-naphthaldehyde (2) and isobutyraldehyde (3) furnished the tetrameric macrocyclic compounds 4 and 6. Detailed NMR-investigations of the acetylated tetrameric species 5 surprisingly support a structure not in agreement with