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Stereospecific5JHH and 6JHH couplings in 3-methyl-3-azabicyclo[3.1.0.] hexan-2,4-dione1

✍ Scribed by C. Dale Poulter; R. Bruce Dickson

Publisher: Elsevier Science
Year: 1971
Tongue: French
Weight: 232 KB
Volume: 12
Category: Article
ISSN: 0040-4039
DOI: 10.1016/s0040-4039(01)96833-9

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✦ Synopsis

The magnitudes of long-range interproton couplings through u bonds or a combination ofa and rrbonds are known in most cases to be geometrically dependent. 2 Although in some instances the correlation between long-range coupling constants and molecular geometry has not been precisely mapped,ze there is growing evi-

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Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.004 A Ê Disorder in main residue R factor = 0.047 wR factor = 0.119 Data-to-parameter ratio = 13.0 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.