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Stereoselective Synthesis of Internal Allylic Fluorides.

✍ Scribed by Sebastien Thibaudeau; Robert Fuller; Veronique Gouverneur

Book ID
101966416
Publisher
John Wiley and Sons
Year
2004
Weight
110 KB
Volume
35
Category
Article
ISSN
0931-7597

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CO-N(Me)OMe X-NH COOtBu 3 CHO 4 2 X-NH COOtBu a) HCl, HN(Me)OMe, BOP, DIEA; b) (OtBu) 3 LiAlH, c) KN(TMS) 2 , CH 3 PPh 3 Br X : Boc, Z n = 1,2 a b c ( )n ( )n ( )n ( )n TETRAHEDRON LETTERS Tetrahedron Letters 42 (2001) 3319-3321