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Stereoselective synthesis of allyl- and homoallylglycines

✍ Scribed by Céline Douat; Annie Heitz; Jean Martinez; Jean-Alain Fehrentz

Book ID
104230527
Publisher
Elsevier Science
Year
2001
Tongue
French
Weight
54 KB
Volume
42
Category
Article
ISSN
0040-4039

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✦ Synopsis

CO-N(Me)OMe X-NH COOtBu 3 CHO 4 2 X-NH COOtBu a) HCl, HN(Me)OMe, BOP, DIEA; b) (OtBu) 3 LiAlH, c) KN(TMS) 2 , CH 3 PPh 3 Br X : Boc, Z n = 1,2 a b c ( )n ( )n ( )n ( )n TETRAHEDRON LETTERS Tetrahedron Letters 42 (2001) 3319-3321

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The fractional distillation of 0-(2-alkenyl or 2-cycloalkenyl) S-alkyl dithiocarbonates (xanthates) affords 2-alkenyl or 2-cycloalkenyl alk'yl