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Stereoselective synthesis of 3,7-diarylaminocholestanes by titanium-mediated reductive amination

✍ Scribed by Ahmad, Md. Wasi; Kim, Hong-Seok

Book ID
126285255
Publisher
Elsevier Science
Year
2014
Tongue
English
Weight
556 KB
Volume
88
Category
Article
ISSN
0039-128X

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## Abstract A practical and selective method for the synthesis of the β‐arylamines 5 and the __cis__‐ or __trans__‐amino alcohols 8 or 11 is reported. The reaction sequence starts from α‐tetralones 1 which readily react with dibenzyl azodicarboxylate to afford the protected α‐hydrazino ketones 2. T