Stationary phase characterization and method development
โ Scribed by Uwe D. Neue
- Book ID
- 102441369
- Publisher
- John Wiley and Sons
- Year
- 2007
- Tongue
- English
- Weight
- 335 KB
- Volume
- 30
- Category
- Article
- ISSN
- 1615-9306
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โฆ Synopsis
Abstract
The properties of stationary phases and their characterization methods are reviewed. New and significant developments have occurred in the last few years, and new methods for stationary phase characterization have become available. The characterization methods are discussed, and the differences between the different methods are pointed out. In addition, method development approaches are reviewed, with special emphasis on recent developments that employ multiple parameters in parallel. Also, the renewed interest of temperature as a tool in method development is surveyed.
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## Abstract Calixareneโbonded stationary phases received growing interest in HPLC as stationary phases with special retention characteristics and selectivity. The commercially available unsubstituted and __p__โ__tert__โbutylโsubstituted Caltrex^ยฎ^ columns have been intensively studied and character
## Abstract Retention characteristics of seven silicaโbased chromatographic columns (Bidentate C18, Silicaโhydride, Spherisorb ODSโ1, Resolve C18, XTerra C18, XBridge Phenyl and Blaze C8 Polydentate) were compared. The columns differ in the character of the support, including silica type B, hydrosi