Synthesis and characterization of titania based stationary phases using the silanization/hydrosilation method
β Scribed by J. J. Pesek; M. T. Matyska; J. Ramakrishnan
- Book ID
- 105586982
- Publisher
- Springer
- Year
- 1997
- Tongue
- English
- Weight
- 961 KB
- Volume
- 44
- Category
- Article
- ISSN
- 0009-5893
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A hydrosilation reaction was used to bind four compounds with one or more alkyne groups or two alkene functionalities. The diffuse reflectance infrared Fourier transform, the 29Si cross-polarization magic-angle spinning (CP-MAS) NMR, and the 13C CP-MAS NMR spectra were used to characterize the vario
## Abstract Chitosan was modified with __N__βnicotinoylβLβphenylalanine and 3,5βdimethylphenylisocyanate to prepare a chiral stationary phase for the high performance liquid chromatography application, especially for the separation of optical isomers of series of Ξ±βamino acids. The modified chitosa