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Stabilization of Lithium Borohydride with Nitrogen Donor, Chelating Ligands. Syntheses and Solid State Structures of [HC(3,5-Me 2 pz) 3 ]Li(η 3 -BH 4 ), {[H 2 C(3,5-Me 2 pz) 2 ]Li(μ-η 3 -BH 4 )} 2 , and {[4,4‘-Me 2 bipy]Li(μ-η 3 -BH 4 )} 2 (pz = pyrazolyl, bipy = bipyridyl)

✍ Scribed by Reger, Daniel L.; Collins, James E.; Matthews, Michael A.; Rheingold, Arnold L.; Liable-Sands, Louise M.; Guzei, Ilia A.

Book ID
126807316
Publisher
American Chemical Society
Year
1997
Tongue
English
Weight
220 KB
Volume
36
Category
Article
ISSN
0020-1669

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📜 SIMILAR VOLUMES

Synthesis and structural characterizatio
Synthesis and structural characterization of a face-sharing bioctahedral complex [HB(Me2Pz)3)BH][Br3Mo(μ-Br)3MoTp*] and an edge-sharing tetramolybdenum complex [Mo4(μ3-O)2(μ2-O)2(μ2-OH)2(O)4(Me2PzH)6](Br)4(Me2PzH2)2 (Tp*=hydridotris(3,5-dimethylpyrazolyl)borate); Pz=pyrazolyl)
✍ Chen-Long Lee; Pang-Yen Yang; Chang-Wei Su; Jhy-Der Chen; Lin-Shu Liou; Ju-Chun 📂 Article 📅 2001 🏛 Elsevier Science 🌐 English ⚖ 151 KB

From a solution prepared by a reaction of Mo 2 (O 2 CCH 3 ) 4 with KTp\* (Tp\*= hydridotris(3,5-dimethylpyrazolyl)borate, HB(Me 2 Pz) 3 ), in diglyme at room temperature followed by addition of excess (CH 3 ) 3 SiBr to the red solution in refluxing THF, the complexes [HB(Me 2 Pz) 3 )BH][Br 3 Mo(m-Br