## Abstract An investigation of bis(diphenylphosphino)methane dioxide (dppm dioxide), __cis__β[PtCl~2~(PPh~3~)~2~] __cis__β[PtCl~2~{P(__p__βC~6~H~4~Cl)~3~}~2~] and __cis__β[PtBr~2~(PPh~3~)~2~] by solidβstate CP/MAS ^31^P NMR spectroscopy, xβray powder diffraction and ^1^H, ^13^C{^1^H} and ^31^P{^1^
β¦ LIBER β¦
Spinning-Frequency-Dependent 31P MAS NMR Spectra of Square-Planar Metal-Phosphine Complexes
β Scribed by Wu, Gang; Wasylishen, Roderick E.
- Book ID
- 127358459
- Publisher
- American Chemical Society
- Year
- 1994
- Tongue
- English
- Weight
- 606 KB
- Volume
- 33
- Category
- Article
- ISSN
- 0020-1669
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Chiral synthons containing either 13Cor 15N-labelled glycine were prepared. The 13C and 15N NMR spectra of the Ni(II) complex of the Schi β base of (S)-2-(N-benzylprolyl)aminobenzophenone and 13C-1-, 13C-2or 15N-labelled glycine were measured and assigned. The observed splitting of the carbon signal