The observation of two-dimensional NMR spectra of crystalline solids. The 31P CP-MAS COSY and J-resolved spectra of a phosphine complex of Hg(II)

Complete assignment of the 13C NMR spect

Complete assignment of the 13C NMR spectra of bleomycin A2 and its zinc complex by means of two-dimensional NMR spectroscopy

✍ M. A. J. Akkerman; C. A. G. Haasnoot; U. K. Pandit; C. W. Hilbers 📂 Article 📅 1988 🏛 John Wiley and Sons 🌐 English ⚖ 757 KB

13C NMR spectra of free bleomycin A, at pH 4 and 6.7 and of its zinc complex at pH 6.7 were completely assigned by making use of two-dimensional 'H-"C correlated spectroscopy. Differences in resonance positions between the spectra of the free bleomycin at pH 4 and 6.7 are observed for the /?-hydroxy