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Spinnability and rheological properties of sols derived from Si(OC2H5)4and Zr(O-nC3H7)4solutions

✍ Scribed by Dae-Young Shin; Sang-Mok Han


Publisher
Springer
Year
1994
Tongue
English
Weight
437 KB
Volume
1
Category
Article
ISSN
0928-0707

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Reaction of [Mo 3 Y(m-S) 3 (dtp) 4 (H 2 O)] (Y O, S; dtp S 2 P(OC 2 H 5 ) 2 Γ€ ) with HgI 2 gave the novel compound {[Mo 3 S 7 (dtp) 3 ] 4 Β΄I}{(HgI 3 ) 3 } Β΄4 H 2 O (1), which contains a {[Mo 3 S 7 (dtp) 3 ] 4 Β΄I} tetramer and (HgI 3 ) Γ€ . Compound 1 has been characterized by IR, Raman, UV/Vis, and N