Sperminium bis(tri-tert-butoxysilanethiolate)–2-propanol (1/2)
✍ Scribed by Baranowska, Katarzyna ;Chojnacki, Jaroslaw ;Wojnowski, Wieslaw ;Becker, Barbara
- Book ID
- 104481243
- Publisher
- International Union of Crystallography
- Year
- 2003
- Tongue
- English
- Weight
- 273 KB
- Volume
- 59
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
Single-crystal X-ray study T = 200 K Mean '(C±C) = 0.005 A Ê Disorder in main residue R factor = 0.035 wR factor = 0.131 Data-to-parameter ratio = 13.7
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📜 SIMILAR VOLUMES
pounds, presumably oligomers. In glacial acetic acid (CH3C0,H/CH2C12=3 :2, i=40 mA/cm2, T=2OoC, Pt electrode) 17% androstanyl acetate is obtained and 38% androstane is recovered. Remarkable is the selectivity of the oxidation: We found that the 6-(6a), 7-, and 12-acetates are formed in the ratio 35