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Spectrophotometric Determination of Baclofen.. Spektrophotometrische Bestimmung von Baclofen

✍ Scribed by Sedat Tosunoǧlu; Nadir Büyüktimkin

Publisher
John Wiley and Sons
Year
1989
Tongue
English
Weight
172 KB
Volume
322
Category
Article
ISSN
0365-6233

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A solution of 2.0 g (0.01 mol) of 1 in 30 ml of DMF was treated with 3.0 ml(0.02 mol) of 2d and stirred at room temp. for 30 min. The precipitate was washed with DMF to give 1.8 g (60 %) of crude product 4, mp. 193-198", vco 1720cm-', mol. mass294 (ms). 1.8 g (6 mmol) 4 was dissolved in 16 ml of gla