triphenylphosphanimino)tetrazolo [5,1-a][1,3,5]tri-An improved crystal structure for 2,4,6-triazido-1,3,5-triazine (2) was determined and for the first time a 14 N-NMR azine (1) was synthesized by reaction of cyanuric azide with triphenylphosphane. 1 is characterized by X-ray structural spectrum was
Spectrofluorimetric determination of dopamine using 1,5-bis(4,6-dicholro-1,3,5-triazinylamino) naphthalene
β Scribed by Wei Wei; Hong-jian Wang; Chong-Qiu Jiang
- Publisher
- John Wiley and Sons
- Year
- 2007
- Tongue
- English
- Weight
- 284 KB
- Volume
- 22
- Category
- Article
- ISSN
- 1522-7235
- DOI
- 10.1002/bio.1005
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β¦ Synopsis
Abstract
A new fluorescent reagent, 1,5βbis(4,6βdichloroβ1,3,5βtriazinylamino)naphthalene, containing two active chlorines, was synthesized by a oneβstep reaction. Under the optimum conditions for the determination of dopamine, the enhanced fluorescence intensity is proportional to the dopamine concentration. The fluorescence intensity was measured at Ξ»~ex/em~ = 400/460 nm, with and without dopamine. The linear range and detection limit for the determination of dopamine were 1.0 Γ 10^β7^ mol/Lβ5.0 Γ 10^β5^ mol/L and 4.0 Γ 10^β8^ mol/L. This method is simple, practical, can afford good precision and accuracy and can be successfully applied to assess dopamine in injections and human serum samples. Copyright Β© 2007 John Wiley & Sons, Ltd.
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