SOME DERIVATIVES OF 2,4-DINITRO-BENZALDEHYDE. 1
✍ Scribed by Lowy, Alexander; Wescott, Blaine B.
- Book ID
- 126275137
- Publisher
- American Chemical Society
- Year
- 1920
- Tongue
- English
- Weight
- 587 KB
- Volume
- 42
- Category
- Article
- ISSN
- 0002-7863
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## Abstract 2,4‐Dinitro‐[7‐^14^C]benzaldehyde (4), a mutagenic substance which may have an unique metabolic activating pathways, was synthesized as a tracer for the detection of adducts of 4 with macromolecules. The preparation was performed in four steps from [7‐^14^C]toluene to give an overall ra
In the title compound, C~13~H~8~Cl~2~N~4~O~4~, the dinitrophenylhydrazone and benzene ring planes are nearly coplanar, making a dihedral angle of 3.39 (9)°. There is an intramolecular N—H...O interaction and weak intermolecular C—H...O hydrogen-bonding interactions which stabilize the packing.