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Solvothermal Synthesis of Nanocrystalline MoS2from MoO3and Elemental Sulfur

✍ Scribed by J.H. Zhan; Z.D. Zhang; X.F. Qian; C. Wang; Y. Xie; Y.T. Qian

Publisher: Elsevier Science
Year: 1998
Tongue: English
Weight: 223 KB
Volume: 141
Category: Article
ISSN: 0022-4596
DOI: 10.1006/jssc.1998.7991

No coin nor oath required. For personal study only.

✦ Synopsis

Molybdenum disulfide crystallites has been synthesized from MoO 3 , S, and N 2 H 4 H 2 O in pyridine at 300°C for 12 h with good yield ('90%). The product is characterized by X-ray powder diffraction (XRD) and transmission electron microscopy (TEM). XRD and IR analysis show that pure MoS 2 has been prepared. TEM shows that these nanoparticles are in the form of platelets. Here, a bi-step transition process from MoO 3 to MoO 2 and from MoO 2 to MoS 2 is proposed.

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