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Solvent-Free N-Alkylation of Phenyl Sulfanilides under Microwave Irradiation.

โœ Scribed by P. Jaisankar; P. C. Srinivasan


Publisher
John Wiley and Sons
Year
2006
Weight
16 KB
Volume
37
Category
Article
ISSN
0931-7597

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Solvent Free Protection of Carbonyl Group under Microwave Irradiation. -The conversion of carbonyl compounds (I) to the corresponding acetals/ketals (III) or dioxolanes (V) is readily achieved by neat KSF clay or PTSA-catalyzed microwave irradiation in the presence of orthoformates, 1,2-ethanediol,