𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Solvent-Free Fmoc Protection of Amines Under Microwave Irradiation

✍ Scribed by Godoi, Marcelo; Botteselle, Giancarlo V.; Rafique, Jamal; Rocha, Manuela S. T.; Pena, Jesus M.; Braga, Antonio L.

Book ID
123610840
Publisher
Wiley (John Wiley & Sons)
Year
2013
Tongue
English
Weight
197 KB
Volume
2
Category
Article
ISSN
2193-5807

No coin nor oath required. For personal study only.

πŸ“œ SIMILAR VOLUMES

Solvent free protection of carbonyl grou
Solvent free protection of carbonyl group under microwave irradiation
✍ Bertrand PΓ©rio; Marie-Joelle Dozias; Patrick jacquault; Jack Hamelin πŸ“‚ Article πŸ“… 1997 πŸ› Elsevier Science 🌐 French βš– 200 KB

Protection of aldehydes and ketones as aoetals or dioxolanes Β’aitalysod by PTSA or KSF clay was readily afhieved from orthoformates, 1,2-ethanediol or 2,2-dimethyl-l,3-dioxolane without solvent under microwave irradiation.

ChemInform Abstract: Solvent Free Protec
ChemInform Abstract: Solvent Free Protection of Carbonyl Group under Microwave Irradiation.
✍ B. PERIO; M.-J. DOZIAS; P. JACQUAULT; J. HAMELIN πŸ“‚ Article πŸ“… 2010 πŸ› John Wiley and Sons βš– 34 KB πŸ‘ 2 views

Solvent Free Protection of Carbonyl Group under Microwave Irradiation. -The conversion of carbonyl compounds (I) to the corresponding acetals/ketals (III) or dioxolanes (V) is readily achieved by neat KSF clay or PTSA-catalyzed microwave irradiation in the presence of orthoformates, 1,2-ethanediol,

Solvent-free thionation of Ξ³-lactones un
Solvent-free thionation of Ξ³-lactones under microwave irradiation
✍ Jean-Jacques Filippi; Xavier Fernandez; Louisette Lizzani-Cuvelier; AndrΓ©-Michel πŸ“‚ Article πŸ“… 2003 πŸ› Elsevier Science 🌐 French βš– 386 KB

A series of g-thionolactones was synthesized, with good yields, using a new combination of Lawesson's reagent (LR) and hexamethyldisiloxane (HMDO) in solvent-free conditions under microwave irradiation.